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Micromorphological analysis of the deposits at the early pottery Xianrendong cave site, China: formation processes and site use in the Late Pleistocene

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ORIGINAL PAPER

Micromorphological analysis of the deposits at the early pottery

Xianrendong cave site, China: formation processes and site use

in the Late Pleistocene

Ilaria Patania1 &Paul Goldberg2,3&David Joel Cohen4&Xiaohong Wu5&Chi Zhang5&Ofer Bar-Yosef1

Received: 22 September 2016 / Accepted: 14 January 2019 # Springer-Verlag GmbH Germany, part of Springer Nature 2019

Abstract

Excavations at the cave site of Xianrendong (Jiangxi Province, China) recovered the earliest known pottery (20/19,000 calBP) in the world from a typical South China Upper Paleolithic chopper–chopping tool assemblage together with bone, antler, and shell tools. Here, we present the results of micromorphological and preliminary FTIR analysis of the deposits looking at high-resolution evidence of site formation processes, stratigraphic integrity, and spatial use of the site. The excavations in the cave can be divided into two areas, east and west. We demonstrate that the contexts of the micromorphological samples from both areas show negligible disturbances within the deposits, thus supporting the stratigraphic integrity of the radiocarbon samples used to date the pottery and site sequence. We also find differences in the formation processes between the east and west areas, including evidence of anthropogenic activities such as usage of hearths and dumping areas and differing geogenic inputs during the depositional history of each area. This study, the first of its kind for a Chinese Upper Paleolithic cave site, demonstrates the advantages of the systematic use of geoarchaeological methods (micromorphology and FTIR) for reconstructing human activities and site use and their environmental contexts.

Keywords Xianrendong cave . Late Pleistocene South China . Upper Paleolithic archeology . Micromorphology . FTIR analysis . Early pottery

Introduction

The Upper Paleolithic (or Late Paleolithic, as called in China) cave site of Xianrendong in Jiangxi province in southern

China (Fig.1) is well known for the discovery of the earliest pottery in the world, from hunter-gatherer contexts dating to 20,000 cal BP(Wu et al. 2012). This karst cave contains a

sedimentological record spanning from ca. 29,000 to 9000 cal BP, with an occupational record of intermittent use of the cave by people for at least 16,000 years, beginning ca. 25,000 calBP(Beijing and Jiangxi2014; MacNeish1999; Wu et al.2012; Zhang2002).

Excavations at Xianrendong reveal a typical South China Late Paleolithic material culture of core and flake tool tech-nology with choppers and chopping tools, as well as some bone and shell tools (Jiangxi1963). Within this assemblage, however, is also pottery (represented by a small number of sherds), first produced by foraging groups using the cave ca. 20,000 calBP, and which today represents the earliest known

example of pottery vessel production (Wu et al.2012; Cohen

2013; Cohen et al.2017). Excavations at the site were con-ducted over five seasons (1962, 1964, 1993, 1995, and 1999) in conjunction with the nearby cave of Diaotonghuan (Beijing and Jiangxi2014, Jiangxi1963,1976; MacNeish and Libby

1995,1999; Zhang2002), but the complexity of the deposits and disagreements over the interpretation of the available

Electronic supplementary material The online version of this article (https://doi.org/10.1007/s12520-019-00788-6) contains supplementary material, which is available to authorized users.

* Ilaria Patania ipatania@bu.edu

1

Department of Anthropology, Harvard University, Cambridge, MA, USA

2 CAS, SEALS, University of Wollongong, Wollongong, NSW 2522,

Australia

3

Institut für Naturwissenschaftliche Archäologie, Eberhard-Karls-Universität Tübingen, Rümelinstr. 23, 72070 Tübingen, Germany

4

Department of Anthropology, National Taiwan University, Roosevelt Rd., Sec. 4, No. 1, Taipei 106, Taiwan

5 School of Archaeology and Museology, Peking University,

Beijing 100871, China

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radiocarbon dates prevented a clear interpretation of the site’s dating and usage. To resolve these issues, collaborative field-work in 2009 (with authors P.G., D.J.C., X.W., C.Z., and O.B.-Y. participating) reopened two earlier trenches (indicated in Fig.1) to clarify chronological and site formation issues by employing a systematic sampling strategy for mi-cromorphological analyses paired with radiocarbon dating (Wu et al.2012). This paper provides new, more complete analyses of the micromorphological samples and the geoarchaeology from the site. These analyses allow us to see how the sedimentary history of the cave, and particularly ep-isodes of flooding within parts of the cave, affected human occupation.

Xianrendong was discovered by Li Yanxian in 1961, with initial excavations of a large area of 41 m2(squares T1–T6; Fig.1) in 1962 and 1964 (Jiangxi1963,1976). Further exca-vations in 1993 and 1995, aimed at investigating the origins of rice agriculture, by a Sino-American project led by Richard MacNeish, Chen Wenhua, and Peng Shifan opened an addi-tional three units of 20 cm × 1 m each in the west (E0–2N4) and three 50 cm × 1 m units in the east (E11N10–12), with the goal of identifying the earliest presence and domestication sequence of rice in China (MacNeish and Libby 1995; MacNeish et al.1998; Zhang1999). In 1999, excavations of another 4.5 m2 in the east (E11N10–12, E10N10–12) were directed by Peking University and the Jiangxi Provincial

Fig. 1 Plan of Xianrendong Cave showing grid from the 1962–2009 excavations. Inset: location of Xianrendong in southern China (modified from Wu et al.2012). Squares E0N4, E1N4, E2N4 show the 20 cm × 3 m area dug in the 1990s (MacNeish and Libby1995,1998). Dark lines indicate theBWestern^ and BEastern^ profiles re-exposed for micromorphological and radiocarbon sampling in 2009. The WP is in a corrected position from as originally plotted in Wu et al. (2012), Fig.1.

We also note that the absolute positions of the western and eastern groups of excavation units each may be off by perhaps 1 m. However, this does not impact the vertical integrity of the two profiles used in this study. Since we are not in possession of the original field notes, and to avoid further conjecture, we have left the plan unchanged. Future work at the cave should field check the units’ positions and rectify the site plan, if needed

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Institute of Cultural Relics and Archeology (Wang et al.2010; Zhang1999). The determination of the dating of the early pot-tery proved problematic for the 1990s excavators (Cohen et al.

2017). Whereas AMS radiocarbon dates from bone and char-coal were acquired during both the 1995 and the 1999 excava-tions (MacNeish and Libby 1995; MacNeish et al. 1998; Beijing and Jiangxi2014), many of the dates were rejected, as chronological interpretations were never tied to studies of the stratigraphy or site formation processes. MacNeish et al. (1998), MacNeish (1999) and Zhang (2002) instead relied on cross-dating to Jomon pottery in Japan to select radiocarbon dates of ca. 12,500BP(uncalibrated) as the most plausible for the earliest pottery because they saw similarities between earli-est Jomon pottery with that from Xianrendong. As a result, the excavators rejected the large number of radiocarbon dates dat-ing before 12,500BP(uncalibrated) that were stratigraphically

associated with the pottery (Cohen et al.2017; MacNeish et al.

1998; Wu et al.2012; Zhang2002).

The 2009 fieldwork was explicitly designed to re-date the stratigraphic contexts of the earliest pottery-containing layers at the site. With a large series of dating samples coupled with micromorphological analysis to test the stratigraphic integrity of their contexts, the 2009 operation was able to produce a new, secure chronology that placed the earliest pottery at ~ 20,000 calBP(Wu et al.2012). The dating results show that

pottery production at the site begins shortly after the Last Glacial Maximum (defined now as Greenland Stadial 3, with dates of 27,540–23,340 cal BP; see Hughes et al. 2013;

Hughes and Gibbard2015) within a hunter-gatherer context and confirms that Xianrendong pottery is the earliest ceramic vessels not only in China but also known globally.

Here, we present detailed results of the geoarchaeological and micromorphological analysis of samples collected at Xianrendong in 2009 from both the eastern (EP) and western (WP) re-exposed profiles (Fig.1). The purpose of this study is to reconstruct site formation processes, and we show how these were different in these separate areas of the cave. We also evaluate the integrity of the deposits paying special atten-tion to the early pottery-containing layers in order to support the validity of the radiocarbon results by demonstrating there would have been no post-depositional movement of the radio-carbon samples.

Site setting and stratigraphy

Xianrendong Cave is situated in a karst landscape typical of South China, with limestone towers and peaks rising over alluvial valleys (Day and Tang 2004; Huang et al. 2013; Ford and Williams1989; Waltham2008; Zhang1989; Zhu and Waltham2004; Zhu et al.2013). The cave entrance which faces southeast, is ca. 64 m above sea level (asl), and is only a few meters above the modern valley floor (Fig.2), and filled

with reddish brown silty clays. The entrance is 14.32 m wide and opens into a large chamber that narrows toward the back. Beyond a smaller, inner chamber, the cave system divides into five corridors that run N–S (Beijing and Jiangxi2014). Wenxi Creek flows eastward toward the cave but turns abruptly northward without presently flowing in front of the mouth of the cave (Fig.2). Two dams and a series of irrigation canals modify the modern course of this waterway in the area close to Dayuan village. From aerial photographs (Fig.3) and topo-graphic maps (Fig.2), it appears that the channel once flowed through the valley south of Xianrendong but has since changed course.

The 2009 fieldwork reopened two trenches from earlier excavations: a western one from the 1993 excavation (north wall profile of E0–3N4, at a balk between it and T4), and an eastern one from the 1995–1999 excavations (west wall pro-file of E10N10–12). Both trenches are situated in the main chamber and are separated by a modern visitor path and a large slab of protruding bedrock covered by roof fall (Fig.

1). For the purposes of this study, these two trenches are la-beledBWestern^ and BEastern^ Profile according to their po-sition within the chamber. A partially excavated block of pro-truding sediment between them is called theBCentral Area^ (Fig.1).

A lengthy description of the stratigraphy was published in the Chinese final excavation report (Beijing and Jiangxi

2014), with a translated and modified version presented in the online resources (see Online Resource1). It is important to note that the 1990s excavators used a separately and inde-pendently numbered stratigraphic sequence for each of the profiles, and also used the same numerical labels for either side; thus, with the exception of Layer 4, there is no correla-tion between layers of the same number from the two systems. In other words, Layer 3A in the WP is not equivalent to Layer 3A (and its subdivisions) in the EP. To avoid confusion, in this report we prepend an area notation to the layers, so that Layer 3A in the WP is BLayer West3A,^ and in the East, BLayer East3A.^

The published descriptions of the stratigraphic layers in the final report for the site (Beijing and Jiangxi2014) were based on field observations done with the naked eye by the Chinese archeologists (Online Resource1). Overall, their observations indicate that the sediment in the WP is composed of a silty-clayey matrix with a coarse fraction of sand-sized grains of quartz, schist, and mica (Fig.4a, c). The lower layers, West4B and West4A, are composed of dark sandy-clay, with limestone and occasional charcoal fragments. Layer West3C2 is a soft but compact sand with large weathered limestone blocks. Layer West3C1B, which contained the earliest pottery, was identified as a reddish brown hard layer with a large quantity of burned clay, charcoal pieces, and weathered breccia. The bottom of this layer exhibits a hard, clay-rich portion that seems unevenly burned. Burned clay fragments are found in

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Fig. 2 Topographic map of the vicinity of Xianrendong Cave (after MacNeish and Libby1995). Wenxi Creek, flowing to the east of the cave, is the only modern watercourse in the immediate surroundings of the site.

However, the capacity and course of the creek have been modified by several dams visible on the map. The valley south of the peak is an ancient alluvial valley that is today occupied by rice paddies

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Layers West3C1A, West3B2, and West3B1 above it; these layers also include limestone fragments and some charcoal.

Our observations in the field indicate that whereas the com-ponents of the WP seem to be consistent from bottom to top, the sediments in the EP vary vertically (Fig.4b, d). One key aspect newly noticed in the field in 2009 was the quantity of mica within the different layers, with this observation support-ed by the micromorphological analysis (see below and Online Resource2). Following the descriptions in the excava-tion report, Layer East5A, near the base, is composed of red-dish brown sandy-clay with coarse sand and some breccia pieces coated in sandy silt. The layers above, East4B and East4A, are composed of dark sandy-clay with limestone

and occasional charcoal. While the early excavators of the site noted that these layers extended to both sides of the cave, we did not find evidence to support this in the re-opened WP. Layer East3B is yellowish brown sandy clay with medium and fine quartz sand and breccia fragments; abundant charcoal pieces are mixed with the upper part of the layer, mostly in the center area. Layer East3A1 is the first one in this profile to be sampled for micromorphology. It is composed of gray silt, with a coarse fraction of sand-sized quartz, feldspar, and small amounts of mica. This layer is sandwiched between bands of coarse gravel ~ 2.5-cm thick. Layer East2B2 is a reddish-brown sandy silty clay with clay clumps. Calcium carbonate concretions and limestone gravel and breccia appear to be

Fig. 3 Aerial view of the area around Xianrendong (indicated by the red dot) showing the alluvial valleys that surround the peak that are today cultivated with rice, Wenxi Creek flowing past Dayuan Village, and the

dams that have modified its channel (from Google Earth). The star marks the alluvial valley in front of the cave where we hypothesize the watercourse discussed in the text originally flowed

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more abundant in the lower part of the layer. The layer is of uneven thickness, and it thins and disappears toward the south. Layers East2B (which contains the earliest pottery) and East2A3 are compact brown sandy-loams with limestone brec-cia inclusions and charcoal. Layers East2A2, East2A1, and East2A are dark sandy clay with limestone breccia inclusions. Layer East2A2 is relatively loose, whereas both East2A1 and East2A are compact. Layer East2B is a dark red sandy-silt with loose structure and abundant angular gravelly inclusions. The original excavators note that this earliest-pottery containing layer did not seem to be disturbed. The uppermost Layer, East1A, is light gray silt with cemented shells.

Chronology and dating

There are no dates nor radiocarbon samples from the 1960s excavations due to the chaos of the Cultural Revolution and the closure of many academic institutions during that period. The excavations in the 1990s with better stratigraphic controls yielded a large series of radiocarbon determinations. However, as mentioned above, MacNeish et al. (1998) chose to select those dates that seemed to match dates of early pottery known from Jomon contexts in Japan and they rejected dates that were earlier. They thus selected only seven radiocarbon determina-tions as acceptable out of 34 samples dated and tried to support this using pollen studies (MacNeish and Libby 1995; MacNeish et al.1998; MacNeish and Libby1999). MacNeish and Libby (1999) explain that they rejected the many dates due to what they perceived as inadequate and poor samples, sup-posed problems with equipment at the Peking University (BA) laboratory not being up to date and reliable, and possible CaCO3contamination of the14C samples. It is clear today that these issues are not relevant anymore (Cohen et al.2017).

The main purpose of the 2009 operation was to clarify the chronology of the layers at Xianrendong, and 45 samples of bone or charcoal fragments each > 1 cm in size were dated (Tables1and2). The bone samples also included faunal re-mains excavated in the 1990s stored at Peking University in addition to those collected from the re-exposed profiles (Wu et al.2012). The criterion for only dating samples of size > 1 cm was based on the micromorphological assessment show-ing samples of this size would not have been moved from original depositional contexts by post-depositional processes. The chronology published by Wu et al. (2012) places the first appearance of pottery at the site at ca. 20,000 calBP, with the

earliest sherds found in Layers West3C1B and Layers East2B and East2B1 (Fig.4a, b). These results confirm as correct the radiocarbon dates produced in the 1990s that were associated with the earliest pottery but rejected by MacNeish.

The 2009 results also provide many more chronological details for the history of the deposits of the cave. First, they show geogenic sedimentation earlier than 29 ka calBP(Layers

East6B and West4A). The nature of human occupation is also shown to be intermittent, occurring between 25,000 calBPand 9000 calBP(Wu et al.2012). The lack of a radiocarbon record

between 17,500 and 14,500 calBP(Wu et al.2012) is difficult to interpret, and could be due to either a period of non-deposition or to erosion of the deposits; it is impossible there-fore to conclude whether the cave was occupied during this time. The micromorphology, as discussed below, also can clarify the in situ nature and stability of the contexts of the radiocarbon samples, and can aid in further reconstructing the depositional and human behavioral contexts for the pottery and other material culture found here.

Methods

This micromorphological analysis of the sediments of Xianrendong Cave is designed to identify their components and their nature and in turn to reconstruct both the geological and human behavioral contexts of the material culture found in the cave. Twenty-four undisturbed sediment blocks were col-lected from the EP and WP (Figs.1and4): samples 1 to 7 are from the WP, and samples 19 to 29 are from the EP (Online Resource2). Samples 9 to 13, determined to be from a backfilled trench, are excluded, and samples 14 to 18, from the upper layers of the central profile, are not studied here, as their stratigraphic placement relative to the other profiles is not clear at present. In both WP and EP, the sediment sample blocks were collected from vertical exposures and include each layer and the boundaries between them (Figs.1and4). After removing the intact blocks, they were wrapped tightly in tissue paper and packaging tape in the field to ensure stability during transport.

At the Micromorphology Laboratory at Boston University, the blocks were oven dried for several days at 60 °C. They were then impregnated with a mixture of 7 parts unpromoted polyester resin and 3 parts styrene catalyzed with methyl-ethyl-ketone-peroxide (MEKP; 8 mL per liter of mixture). Once the resin had gelled, the samples were placed in the oven overnight at 60 °C to complete the process. After impregna-tion, representative areas were selected for petrographic thin sectioning; in the case of long blocks, two parts were chosen (labeled A, upper; and B, lower). The blocks were trimmed with a rock saw to produce 50 × 75 × 10 mm chips that were sent to Spectrum Petrographics (Vancouver, WA, USA) for processing into thin sections. To facilitate μ-FTIR analysis (see below) the slides were left uncovered.

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Fig. 4 a Xianrendong WP with locations of the micromorphology samples indicated. b Xianrendong EP with locations of the micromorphology samples indicated (modified from Wu et al.2012). c Photo of the WP with locations where block samples were removed indicated. d Photo of the EP with locations where block samples were removed indicated

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The petrographic thin sections were scanned on a flat-bed scanner at 2400 dpi with the lid open producing aBdark field^ (Goldberg and Aldeias2018). The thin sections were examined using a microfilm reader, and binocular and petrographic mi-croscopes in plane-polarized light (PPL), cross-polarized light (XPL), and oblique incidence light (OIL) at various scales from × 5 to × 200 (Courty et al.1989). Descriptive nomenclature follows that of Stoops (2003) and Courty et al. (1989).

In order to identify and quantify the effects of heating, fragments of bone and clay aggregates in the thin sections were analyzed by μ-FTIR (Fourier Transform Infrared Spectroscopy microscope) at the Center for Archeological Science at the University of Tübingen using an Agilent Technologies Cary 600 series FTIR machine equipped with a Cary 610 microscope. The spectra were recorded directly on the thin sections using transmitted and attenuated total reflec-tance (ATR) mode fitted with a Germanium crystal (see Berna et al.2007; Berna and Goldberg2007; Simms et al.2013).

Table 1 Radiocarbon determinations from Xianrendong WP Laboratory number 14 C Date (Libby half-life) Calibrated age range yearBP1σ Material Layer West2A BA09891 10,210 ± 50 11,914 ± 139 Bone Layer West3A BA09894 12,240 ± 55 14,305 ± 254 Bone Layer West3B1 BA093181 14,610 ± 290 17,869 ± 473* Charcoal Layer West3B2

UCR3561 12,420 ± 80 14,653 ± 350* Human bone Layer West3C1A BA09872 14,235 ± 60 17,448 ± 252 Bone BA09868 14,925 ± 70 18,218 ± 244 Bone BA09875 13,885 ± 55 17,128 ± 195 Bone BA09874 15,165 ± 55 18,319 ± 257 Bone BA00006 15,655 ± 194 18,928 ± 272 Bone UCR3562 16,010 ± 70 19,153 ± 220* Human bone BA95143 16,340 ± 200 19,577 ± 389* Charcoal Layer West3C1B BA10264 16,165 ± 55 19,283 ± 253 Bone BA10266 16,485 ± 55 19,801 ± 301 Bone UCR3439 16,730 ± 120 19,965 ± 305* Charcoal BA00007 16,915 ± 186 20,177 ± 356 Bone AA15005 17,420 ± 130 20,867 ± 318* Charcoal UCR3440 18,520 ± 140 22,120 ± 335* Charcoal Layer West3C2

UCR3300 15,180 ± 90 18,327 ± 264* Human skull UCR3522 17,580 ± 80 20,986 ± 318* Charcoal BA09878 17,915 ± 80 21,542 ± 349 Bone BA00008 17,983 ± 177 21,671 ± 430 Bone BA93182 18,110 ± 270 21,788 ± 449* Charcoal Layer West4A BA00009 22,902 ± 322 27,294 ± 486 Bone BA09880 24,080 ± 95 28,885 ± 378 Bone Dates marked with an asterisk are from MacNeish and Libby (1995). Layer West3C1B contained the earliest pottery in this section. Laboratory codes: BA = Peking University Radiocarbon Laboratory; UCR = University of California, Riverside Radiocarbon Laboratory; AA = NSF-Arizona AMS Laboratory, Tucson. Ch indicates a charcoal sample (after Wu et al.2012). Dates calibrated by CalPal-HULU.2007 version, 1-standard deviation (from Wu et al.2012)

Table 2 Radiocarbon determinations from Xianrendong EP Laboratory number 14C Date (Libby half-life) Calibrated ageBP1δ Material Layer East2A BA00004 10,456 ± 118 12,354 ± 220 Bone BA95138 11,840 ± 150 13,772 ± 212* Charcoal Layer East2A1 UC-R3558 11,020 ± 60 12,927 ± 105* Human bone BA99038 11,840 ± 380 13,950 ± 543 Bone Layer East2A2 BA09899 16,330 ± 65 19,557 ± 270 Bone Layer East2A3 BA95139 16,110 ± 140 19,247 ± 267* Charcoal Layer East2B1 (earliest pottery)

BA10263 16,030 ± 55 19,166 ± 219 Bone BA09912 16,495 ± 60 19,811 ± 303 Bone Layer East2B (earliest pottery)

BA09902 16,095 ± 65 19,215 ± 230 Bone BA10268 16,270 ± 65 19,449 ± 310 Bone BA00015 16,301 ± 157 19,499 ± 350 Bone BA99037 16,330 ± 220 19,563 ± 409 Bone BA09926 16,345 ± 70 19,581 ± 267 Bone BA95141 16,580 ± 260 19,858 ± 376* Charcoal BA10271 17,105 ± 60 20,467 ± 352 Bone BA95140 17,460 ± 210 20,902 ± 358* Charcoal Layer East3A BA95142 20,940 ± 440 25,077 ± 629* Charcoal BA09921 21,820 ± 85 26,175 ± 424 Bone Layer East4 BA00003 19,634 ± 186 23,433 ± 387 Bone BA95144 21,090 ± 660 25,315 ± 900* Charcoal Layer East6B BA99039 24,500 ± 370 29,298 ± 606 Bone Dates marked with an asterisk are from MacNeish and Libby (1995). Layers with the earliest pottery are East2B1 and East2B (after Wu et al.

2012). Laboratory codes: BA = Peking University Radiocarbon Laboratory; UCR = University of California, Riverside Radiocarbon Laboratory. Ch indicates a charcoal sample. Dates marked with an aster-isk are cited by MacNeish and Libby (1995). Dates calibrated by CalPal-HULU.2007 version, 1-standard deviation (from Wu et al.2012)

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Transmitted mode was used for the mineralogical analysis of clays recording wavenumbers between 4000 and 2000 cm−1. The Germanium ATR crystal was used for the mineralogical analysis of bone between 2500 and 600 cm−1wavenumbers.

Results

Micromorphological analysis

Microscopic observations of the sample thin sections reveal variations in organization, texture, and fabric of the main con-stituents of the sediments. The basic components of sand, clay, and mica are generally uniform within each individual profile, although their microstructure, organization, and percentage vary both vertically and horizontally. In the following sec-tions, we highlight the key features of the micromorphological observations. Details are illustrated in Online Resource2and in Figs.5–18. As there are significant differences between the EP and WP, we report on the micromorphological content of each profile separately.

Western profile

Micromorphological analysis (Online Resource2) shows that the sediments in the WP are overall uniform in composition, texture, and fabric from bottom to top. The sediments can be differentiated into layers based on differences in the relative quantities of each component and the void patterns (see be-low), with the 1990s field archeologists relying primarily up-on visible differences in the quantities of silts and clays to divide the sediments into the different archeological layers that we continue to use in this study. The sediments have a silty-clay matrix with a coarse fraction of sand-sized quartz and mica, along with some sporadic fragments of schist, which when weathered, liberate mica into the matrix. Post-depositional features include redoximorphic features, such as Fe–Mn mottling and nodules formation (Figs.5 and6) and secondary carbonate features, secondary CaCO3cementation, and needle-like CaCO3coatings and infillings in root passages and fissures (Fig.6) (see Durand et al. 2010; Lindbo et al.

2010; Vepraskas et al.1994). Localized clay fissure infillings (Fig.7) and hydromorphic clay hypocoatings are also frequent and are found in relation to clay depleted groundmass (Fig.8). These features imply water moving through the sediments.

Subrounded clayey aggregates are also present, but in low numbers (Fig.9). These aggregates are opaque due to the high Fe–Mn content and when analyzed with μ-FTIR do not show signs of having been heated (see Online Resource3). We observed only a few isolated fragments of partially phospha-tized limestone. These likely originated further back in the cave, but their origin and mode of transport are not clear, and their frequency is so low that we do not discuss them

further here. Small fragments of bone and small mammal teeth—which occur in very low abundance—are found in most samples (Fig. 10), with the exception of samples 1A, 2B, and 2A (Layer West4B). Humified plant material is pres-ent throughout the profile. The general scarcity of bone, ash, and charcoal in the sediments underlines the general lack of anthropogenic inputs in the deposits of the WP.

Overall, the sediments in the WP are massive, very com-pact, and with little or no bioturbation (see Online Resource2) (Fig. 11). Exceptions were noticed in sample 3A (Layer West4A), which has a subangular-blocky structure, and sam-ple 1A (Layer West4B) and possibly samsam-ple 6 (Layer West3C1B), which exhibit planar lenticular fissures (Fig.12) consistent with ice-lensing (Van Vliet-Lanoë et al.1984; Van Vliet-Lanoë 1987). We also observed clay depletion hypocoatings (Fig.8) and infillings (Fig.7): these are formed when percolating water removes clay from the groundmass, redepositing it in the voids. Calcitic coatings and recrystal-lized calcite (Fig.6) are also present. Redoximorphic features, s u c h a s F e–Mn depletion hypocoatings, Fe–Mn quasicoatings, and Fe–Mn mottling and nodules (Figs.5and

6) are present in every sample. Mottling and staining are for the most part small but very frequent, suggesting short periods of water stagnation. The Fe–Mn redoximorphic features seem to always postdate the calcite (Fig.6), being superposed on the groundmass and the calcitic features. Water saturation of the sediments in the cave is still occurring today: during our field-work in 2009, we observed the bases of both trenches being filled with ~ 40 cm of standing water due to a rise in the water table following a rainstorm (Fig.13).

Eastern profile

Micromorphological results show that in contrast to the WP, which mainly features uniform composition and organization, the sediments in the EP vary vertically (Online Resource2). Throughout the profile, both the fine and the coarse fraction include geogenic as well as anthropogenic materials. The fine fraction is mainly composed of a silty-clayey matrix with abundant ash crystals that have been recrystallized (Fig.14). The coarse fraction is composed of limestone fragments, quartz sand, schist fragments, and low amounts of mica. As in the WP, some slides have visible fragments of weathered schist, which supplies mica to the matrix. The amount of mica remains uniform across all layers in the WP, whereas in the EP the quantity of mica in different layers fluctuates. In particular, the quantities of mica diminish upwards between samples 19 through 24 (Layers East3A1 and East2B), coinciding with a change of fabric and microstructure in these samples. Samples 19A and 19B (Layer East3A1) are more compact, showing some diffuse bedding, and they contain more mica and no evidence for anthropogenic input (Fig.15a). Layer East3A1 is similar to the sediments observed in the WP. Changes in

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texture, composition, and fabric occur mostly between sam-ples 19 and 20 (Layers East3A1 and East2B2) and between 20 and 24 (Layer East2B) (Fig.15a–c). Samples 20 to 22 (Layer East2B2) do not show diffuse bedding; instead, they have a complex and open microstructure with no specific arrange-ment of the components, and are relatively porous expressed by large fissures, chambers, and vesicles (Fig.15b, c). These samples contain significantly less mica than the sediments in the layer below (East3A1), but contain large bone fragments, ash that has been recrystallized (Fig.14), and occasional char-coal. The samples in the upper layers, 24 (Layer East2B) to 28 (Layer East2A), are more compact with lower porosity com-posed of fissures, chambers, and vesicles (Fig.15c). The com-ponents are composed of unoriented silty clay, quartz sand, large limestone fragments, very low to no mica, recrystallized ash, heated bone fragments, and charcoal (Fig.16).

Unlike the WP, the EP contains clear evidence of human input. Abundant bone was found throughout the profile

(Fig.16), some of which show features consistent with fish bones. Most bone fragments show evidence of having been exposed to heat (Fig. 16a, b) by their darker color. Furthermore, some of the bone fragments exhibit unusual in-terference colors due to diagenetic processes that are currently being investigated. In addition to bone, other anthropogenic components include fragments of charcoal and ashes (Fig. 16c). Several fragments of freshwater mollusks were observed, but it is not clear whether they are anthropogenic or are of alluvial origin (see below).

Clay aggregates are present throughout the EP and in higher amounts than in the WP. The few clay aggregates found in samples 19 and 20 show indistinct or randomly striated b-fabrics (see Stoops2003); however, most clay aggregates in samples 21 to 29 above these are isotropic.

Post-depositional processes are more frequent and evident in the EP. Samples throughout the profile also contain Fe–Mn orthic nodules, mottling, and hypocoatings (Fig. 17a, b). These redoximorphic features, which form in waterlogged environments, are consistent with the localized clay coatings and intercalations. Layer East3A1 (samples 19B and 19A) (Fig.15) is compact with few signs of bioturbation. The sed-iments in Layer East2B2 (samples 20, 21, 23, 29, and 22B) (Fig.15) have a subangular to angular structure. However, it is important to note that the space between the peds never ex-ceeds 5 mm in width and that within the peds the matrix is quite compact (Fig.15). Layer East2B2 is the most affected by bioturbation, while the layers above are quite massive and cemented by secondary calcite probably derived from the dis-solution and re-precipitation of ash (Fig.17c, d), as is sug-gested by the relicts of ash rhombs in the matrix (Fig.14). Microcrystalline calcite can be observed in the voids as well as in the matrix (Fig. 17c, d). However, some bioturbation caused by earthworms and land snails is visible in the upper layers where passages are up to 9 mm in diameter.

In sum, the micromorphological results show the follow-ing features: The WP has a uniform composition of a silty

Fig. 5 Fe–Mn oxide hypocoating (orange arrow) and some Fe–Mn mottling (blue arrow) in a sandy-clay matrix in Layer West4A (sample 3A, OIL). Fe–Mn redoximorphic features like these can be found throughout the profile and are evidence for a waterlogged environment

Fig. 6 Secondary micritic coating of a fissure (white arrows) in Layer West3C2, sample 5A. a XPL, b OIL. Note the Fe–Mn hypocoating (or-ange arrows) and Fe–Mn mottling and nodule formation (blue arrows).

Deposition of secondary calcite is due to evaporation of carbonate-rich waters that percolate through the sediments through voids

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clayey fine fraction with mica- and quartz-rich coarse frac-tion. Clayey intercalations and infillings and clay-depleted matrix are frequently observed features (Fig.17e). The sed-iment is consistently massive and compact with some len-ticular fissures in Layer West4B. Similar components and microstructures are visible in the lower strata of the EP, but composition and arrangement of the constituents change in the east starting with Layer East2B2, where amounts of mica diminish though ash, bone, and clay aggregates are abundant. Whereas the lower EP layers are massive and compact, Layer East2B2 has a subangular to angular struc-ture and the layers above are more crumbly. Some bioturba-tion is visible in Layer East2B2 and above in the form of earthworm passages, but these never exceed 9 mm in diam-eter. Re-precipitated calcite is present throughout the EP as are Fe–Mn nodules and mottles (for a complete list and description of the layers seeOnline Resources).

Discussion

The micromorphological analysis of the samples from the EP and WP demonstrates several key dissimilar aspects of the deposits in these two different areas of the cave. These reflect differences in the sources and agents of deposition, as well as post-depositional processes such as bioturbation. Below, we discuss these differences and highlight site formation process-es at Xianrendong. The rprocess-esults of our study create a clearer history of the human occupation of the cave through the iden-tification of repeated sedimentary patterns that signal specific human activities there, such as cleaning fire features and dumping fire refuse.

Depositional processes

Micromorphological study along with field observations pro-vide insight into the depositional processes at Xianrendong. It is reasonably clear from the components and their arrange-ment that the deposits in the western part of the cave are of alluvial origin, while those of the EP are more complex, with both geogenic (alluvial) and anthropogenic deposits. In the WP, repeated low-energy flooding episodes were associated with a watercourse that we hypothesize ran in front of the cave in ancient times, and that sometimes invaded the cave (Fig.3), resulting in slackwater deposits rich in micaceous clay (see Huang et al.2012). This inference is supported by the occur-rence of clay coatings and clay-depleted coarse fraction quartz domains connected to locally bedded and better sorted coarse fraction, such as in Samples 5A, 5B, and 19B (Figs.7and8) (Brammer1971). The alluvial origin is also suggested by the presence of rounded clay rip up clasts and disorthic Fe–Mn nodules (Samples 2a, 2b, and 4) (Fig. 9). Although

Fig. 7 Horizontal clay intercalation, Layer West3C2 (sample 5B PPL) produced syndepositionally as a slurry with the coarser material

Fig. 8 a Clay coatings and intercalations (yellow arrows) in relation to clay depleted groundmass (orange arrows) in Layer West3C2 (sample 5A PPL). Water moving through the sediments will wash out clay and

concentrate it elsewhere. b Same area shown in OIL to highlight the different colors between the clay coatings and hypocoatings, which appear as bright orange, and the depleted groundmass (sample 5A OIL)

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archeological material was recovered in the WP during exca-vations, micromorphological observations furnish very limit-ed evidence for anthropogenic inputs. Only a few fragments of bone were observed and most do not show any sign of heating (Fig.10). The details highlighted here indicate a presence of human input within an overall low energy fluvial regime: however, the nature of the human occupation in the western side of the cave is not clear yet.

The depositional processes of the sediments in the EP are more complex. The lower layers of the EP—Layers East6A/ 6B to 3A1 (Figs.15and17)—were deposited by water, likely

by the same alluvial processes observed in the West. This is indicated by the radiocarbon chronology, the consistent pres-ence of compact silty clay layers with mica and schist ob-served in the field, and the clay intercalations and clay-depleted domains, compact matrix, and mica observed in thin section (Figs.15and17). Thus, just as in the WP of the cave, the compact micaceous sandy clays in the EP were deposited

by low energy floods that appear to have invaded the entire cave vestibule (Fig.4b). Layer East3A1, the lowest layer for which we have micromorphological samples in this area, con-tains clear evidence for ephemeral anthropogenic occupation (e.g., ash clumps and micro-charcoal) interbedded with geogenic alluvium. The mixed arrangement of the anthropo-genic sediments (bones, ash, and charcoal) point to an original source of a combustion area, but their chaotic arrangement here suggests that this is reworked hearth refuse that was dumped on this side of the cave (Samples 23, 29a, 29b; Online Resource2). Layer East2B2—composed of sandy clay

with visibly less mica than the layers below—is the lowermost deposit to contain consistent anthropogenic inputs, with abun-dant burned bone, ash, charcoal, and heated clay. We found no evidence of occupational floors or surfaces, again suggesting that Layers East2B, 2A2, and 2A1 represent dumped material (see Macphail and Goldberg2010; Schiegl et al.2003). Based on the form of the cave and overall context, it is likely that the

Fig. 9 Subrounded clay aggregate from the WP, Layer West3C2 sample 5B. a PPL. b XPL. Clay aggregates are abundant in the EP but few are found in the WP. The aggregate shown here, composed of clay and silt

size quartz, is dark due to oxidization of Fe–Mn and was not heated, as shown by FTIR, below. This trend suggests that the clay aggregates are geogenic in nature and are not connected to the pottery found in the cave

Fig. 10 Unheated tooth and bone matter, Layer West3C2. a Fragment of a small mammal tooth likely part of the natural cave components (sample 5B, PPL). b XPL photomicrograph of bone fragment (sample 5B, XPL)

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source of these combusted materials was not at this location nor inside the cave itself, but rather originated outside the strict confines of the cave (see below for a more comprehensive discussion on the chronology of the strata).

Bioturbation and diagenesis

Identification and interpretation at Xianrendong of post-depositional processes in general and bioturbation in particular are critical to a holistic understanding of the archeological and geological record. As shown above, there are only local, small bioturbation features in both profiles. This observation strongly supports the chronology proposed by Wu et al. (2012) for the ca. 20,000 calBPappearance of pottery at Xianrendong by minimizing the effect of any move-ment of centimeter-sized objects such as bone that were used in dating. The WP is composed of consistently massive and compact sediments with little porosity and an absence of pedality and bioturbation. Together, they all signal that the artifacts, bones, and charcoal found here were not displaced post-depositionally.

Some features, however, can be used as climatic signals. In the lowest sample (Layer West4A), lenticular fissures were observed and are possibly related to occasional freezing and thawing (see Van Vliet-Lanoë et al.1984; Van Vliet-Lanoë

1987). In addition, Fe–Mn crusts, staining, and orthic nodules

are found throughout the profile and suggest periods of stag-nant water in the cave throughout its history (see Figs.5,6,13,

14, and17a, b). Such chemical features supported formation of syndepositional intercalations and some clay coatings: these are linked to periodic flooding (see Brammer 1971). However, we note that in Layer West3C2, for example (Fig.

6), Fe–Mn precipitation can locally postdate the formation of

clay coatings. The cave was not water saturated for long pe-riods of time since the Fe–Mn features are not well developed. Instead, we should imagine the occurrence of both dry and wet periods during the accumulation of the WP.

The EP, on the other hand, contains more evidence for bioturbation and diagenesis. Bioturbation, although not prevalent, is present in the form of insect or earthworm passage features with a maximum diameter of 9 mm. It is

Fig. 12 Scan of upper portion of sample 1A (Layer West4B) at the base of the profile. The top part has a lenticular microstructure. These features are consistent with frost action and suggest that these lowermost deposits’ sediments underwent some freeze–thaw. The rarity of these features in the sediments at Xianrendong overall suggests that freezing temperatures were an exceptional occurrence here

Fig. 11 Scan of sample 3A showing compact and massive microstructure in Layer West4A. Notice the Fe–Mn hypocoating (orange arrow), which is evidence of periodic water saturation (see also Fig.5)

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important to note that these millimeter-sized features are not pervasive enough to result in large-scale mixing of sediments from different layers or in movements of ob-jects such as bones of the size used in dating. As men-tioned above, the samples from Layer East2A2 have a subangular to crumbly structure. As was the case for the WP, the EP shows evidence of post-depositional water saturation as well as dry periods. In fact, Fe–Mn orthic nodules and staining occur throughout the profile having been produced by saturation from rises in the water table.

The EP is strongly cemented by calcium carbonate. The process of dissolution and crystallization of calcite in caves is a complex one requiring specific conditions and a delicate balance between water precipitation and evaporation, and amounts of CO2(see Holland et al.1964; White2007). The cementation at Xianrendong is probably the result of a fluctu-ation between wet and dry periods, with CO2-rich water dis-solving ashes from layers that are ash rich, and the drying process resulting in the precipitation of dissolved carbonates. Lenticular microstructures, produced by occasional low temperatures that caused the presence of localized ice in the sediments, can be observed in the top portion of sample 20 and possibly 29A (both from Layer East2B2). No other evi-dence for low temperatures was found in the EP. However, at the Hongguang sand dune in Pengze, ca. 180 km north of Xianrendong cave, interbedded layers of eolian sand beds and thin paleosols formed between 26,000 and 20,000BPwere

identified, indicating localized fluctuations, between humid-wet and cold-dry environment (Liu et al.1997). Occasional freezing temperatures during the deposition of Layer East2B2 are therefore not to be excluded at Xianrendong.

Our field observations also reveal a clear erosional gap expressed in a truncation at the western end of Layers East2B2, 2B, and 2A2. It is difficult at the moment to infer the mode of erosion of these layers. However, particularly with the radiocarbon chronology, we can assert that the timing of erosion must have been either before or contemporaneous with the deposition of Layers West3C2, 3C1B, and 3C1A in the WP (Fig.4; Tables1and2).

Furthermore, our analysis of the post-depositional process-es visible in both the Wprocess-estern and the EPs of Xianrendong clearly shows that any archeological materials greater than

Fig. 13 Photo of trench of WP filled with groundwater that had risen after a rainstorm during the 2009 season. Most of the post-depositional features found in the WP are associated with periods of stagnant water like the one shown here

Fig. 14 Silty clay matrix with ash rhombs that have been recrystallized (white arrows) and some Fe–Mn staining (blue arrows) in Layer East2A3 (sample 22B). The middle and upper layers of the EP contain abundant bone, charcoal, and ash. Although the ash is mostly recrystallized (green arrow), often resulting in micritic cementation of the matrix, pseudo-morphs of ash rhombs are still visible at higher magnification (white arrows)

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Fig. 16 Bone fragments in Layer East2A3 and East2B2 with evidence of heating (samples 24 and 29). Most bone fragments in layers 2B2 and above show signs of having been heated. a Bone from Layer East2A3 (sample 24). The light to dark brown color in the PPL photomicrograph suggests that this fragment was heated. b XPL image of the same

fragments also shows features connected to heating such as high birefringence of the bone and some micritic calcite in the pores (green arrow). c Fragmented bone and charcoal in Layer East2B2 (sample 29A). While the field profile exhibited large pieces of bone, fragmented bone in the sediments shown here is consistent with trampling

Fig. 15 Macroscans of samples representative of the changes in the overall texture, composition, and fabric of the different layers from the EP. a Sample 19B from Layer East3A1, showing a compact microstructure with diffused bedding. b Sample 20 from Layer East2B2, showing bones and a complex microstructure with some

angular to subangular peds, localized crumbly, compact, and vughy microstructure. Layer East2B2 contains some roof fall, which may have altered the microstructure. c Sample 24 from Layer East2B is more compact. Here, the components are not arranged in any specific way

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Fig. 17 Examples of some of the post-depositional features observed in the EP. a OIL photomicrographs of Fe–Mn vein like precipitation (blue arrows) in Layer East3A1 (sample 19B). Redoximorphic features appear in sediments after 2 to 3 days of water saturation (see text for discussion), and their presence here suggests that the sediments were waterlogged for short periods of time. b OIL photomicrograph of Fe–Mn mottling and nodules (blue arrows) and clay coatings and infillings (yellow arrows) in Layer East3A1 (sample 19B). Clay can be transported and redeposited by water percolating through the sediments under conditions such as slack water or dripping water. The Fe–Mn hypocoatings and nodules are

superposed on the clay coatings, indicating that they post-date the forma-tion of the clay coatings. c CaCO3depletion (red arrows), infillings of

fissures with recrystallized CaCO3, and cementation of matrix with

micritic carbonate (green arrows) in Layer East2B2 (sample 20). d Same area, shown in OIL to highlight the presence of faint Fe quasicoatings in the calcitic portion. Recrystallization of calcite takes place under wetter conditions. e Clay intercalations (yellow arrows) in Layer East3A1 (sample 19B), which are thought to form in waterlogged environments (Stoops et al.2010) as supported by the presence here of Fr–Mn mottling

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1 cm in size deposited in the sediments in both profiles accu-mulated with the surrounding sedimentary matrix and did not undergo significant post-depositional movement. The biotur-bation that we observe, which is mainly due to disturbance by earthworms and insects, would not have been able to dislocate materials of this size. This strongly supports the contextual integrity of the samples used for radiocarbon dating by Wu et al. (2012). Our results can therefore offer confirmation of the security of the dating of Xianrendong and in particular the dating of the lowest pottery-containing layers from each pro-file to ca. 20,000 calBP, making the sherds found the earliest examples of pottery vessels yet recovered.

Chronology of sedimentation and human use

of the cave

A time–depth plot (Fig.18a, b) reveals changes in the rate of sedimentation, with periods of non-deposition or erosion and periods of more rapid and conspicuous sediment input. Cross-referencing the data from the WP and the EP, we can recon-struct the overall sedimentological history of the cave and identify a few inconsistencies in the dating.

As previously stated, the WP is composed entirely of vial slackwater deposits. The radiocarbon dates point to allu-vial sedimentation between ~29,000 and 27,000 cal BP.

Moreover, the scatterplot (Fig.18a) highlights a hiatus in ac-cumulation in the WP between ~ 27,000 and 21,000 calBP,

thus suggesting either a lack of flooding and/or period(s) of erosion. This hiatus in sedimentation could be due to a shift in the course of or to the disappearance of the watercourse that previously flooded the cave depositing slackwater sediments. Sedimentation starts again between ~ 21,000 and 18,000 cal

BPand continues until ~ 11,000 cal BP(Layers West3C2 to

3A). The micromorphology confirms the reappearance of al-luvial deposition within the upper layers of the WP (Layers West3C2 and above). The cycles of the disappearance and reappearance of water courses near the cave could be connect-ed to localizconnect-ed climatic shifts that were also observconnect-ed at the Hongguang sand dunes between 26,000 and 20,000BP(Liu et al.1997) (see above) or could simply represent lateral mo-bility of the stream channel. To better understand the local paleoclimate and water channel cycles, a more in-depth study of the landscape around the cave is necessary with particular focus on the alluvial valley in front of the cave.

In the EP, the micromorphological data for Layers East6A to 3A1, deposited between ~ 29,000–26,000 cal

BP, show regular sedimentation that is tied to alluvial

in-put. The layers deposited after ~ 26,000 cal BP (from Layer East3A1 upward) are anthropogenic, in contrast to the WP. Thus, for ~5000 years, until ca. 21,000 cal BP,

sedimentation in the cave appears to occur only in the EP,

in response to regular human contributions. At 21,000 cal

BP, alluvial inputs reappear and seem to continue until ca. 11,000 cal BP. This reappearance of the alluvium at

21,000 calBPin the WP and the deposition of the alluvial

Layers West3C2 and 3C1B could be connected to the erosional surfaces and truncations noted in Layers East2B2, 2B, and 2A2. Moreover, the consistent dates of these strata across both profiles point to contemporaneous deposition for these alluvial layers in the west and anthro-pogenic layers in the east. We propose that between ca. 21,000 and 18,000 cal BP, the western portion of the cave was periodically inundated by slackwater. Although there is no micromorphological evidence of human occupation of this part of the cave, stone tools and pottery fragments were recovered here, denoting a possible human presence. However, the nature of the human occupation is still ob-scure in the west. The sediments in the eastern part do not show traces of alluvial input. We also hypothesize that sediments in the east remained untouched by water enter-ing the western side of the cave either because the de-posits were already above the water level or because of other physical barriers not visible today. Only the south-ern and westsouth-ern edges of the eastsouth-ern strata seem to have been impacted by flooding, which caused some erosion and truncation (Layers East2B2, 2B, and 2A2).

While the dates of the pottery at Xianrendong are gen-erally accepted, Kuzmin (2013, 2015) disputes the accu-racy of the ~20,000 cal BP date for the earliest pottery. Although we do not discuss this issue here (see Cohen et al.2017), it is important to mention that our reconstruc-tion signals that one date from Layer East3A1 (26,175 cal BP [BA09921]) is a likely outlier (see Online Resource

4). Whereas we do not have a definitive explanation for its greater age than other samples in this layer, we may hypothesize that this could be related to possible human occupation on older alluvial sediments that existed outside the cave. In other words, it is possible that this radiocar-bon sample was originally present in older sediments out-side the cave and transported inout-side by humans along with other refuse materials that were being dumped in the interior portion of the cave at the time of deposition of Layer East3A1. This radiocarbon date would therefore point to earlier human activity outside the cave and not the date of the later discard activity that coincided with the true date of the deposition of the layer inside the cave. Our reconstruction shows that the rest of the dates published by Wu et al. (2012) are in sequence and con-sistent with the intact stratigraphic order. These data, in-cluding the evidence for the absence of significant biotur-bation, confirms the legitimacy of the ~ 20,000 calBPdate

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Human occupation of the cave and use

of space

The reconstruction of the site formation processes and the chronology of the sedimentation of Xianrendong provide greater insight into the occupational history of the cave. First, the lack of anthropogenic deposits indicates that human use of the cave prior to 27,000 calBP is very ephemeral. Although we cannot confirm that humans visited the cave seasonally, occupation of the cave had to take into account the floodwaters that often invaded it. With the interruption of flooding events at 27,000 calBP, likely related to movement of the river away from the cave, human occupation of the Xianrendong site becomes more conspicuous.

Second, although previously not realized, our data suggest that humans used the space in the eastern part of the cave as a dump where refuse composed of cleaned hearth features and other archeological material accumulated (Samples 22b, 23, 29a, 29b; Online Resource2). Third, as primary human activ-ities appear to be quite limited inside the cave proper, and because no intact living floor has been identified inside the cave vestibule, it is likely that the main human occupation at the site occurred in an unexcavated area outside of the cave, beyond the current drip line at the entrance. If this is the case, then old alluvial sediments from this area could have occa-sionally gotten mixed with the anthropogenic trash dumped in the cave. Unfortunately, the area outside the cave was never excavated or tested, as small buildings were present outside the cave entrance from the original excavations in the 1960s through 1990s. It is not clear if these buildings may have disturbed prehistoric contexts. The buildings were removed in recent years in order to establish a site park, visitor path, and railing close to the cave, but excavations outside the cave were never carried out. Our hypothesis for the main location of human activity at the site being outside the cave should be tested in the future.

Conclusions

The micromorphological study of the sediments of Xianrendong cave reported here demonstrates the potential

of this approach to reveal the nature of geogenic processes and human activities at the cave: through these, we gain deeper understanding of the human behavioral patterns that led to the deposition of cultural remains in the cave. In light of the evidence for flooding and dumping presented here, previ-ous assumptions concerning human habitation within the cave vestibule need to be reconsidered. While it had long been assumed that people were living inside the cave, our analysis shows no presence of occupational surfaces. These locations only contain refuse that was dumped in the cave but reveal no evidence for the primary activities that created such waste products. The micromorphological analyses coupled with ra-diocarbon dates reveal the increasing presence of human ac-tivity in the cave coinciding with the still cold period just after LGM (~ 20,000 calBP). This is the period when the earliest pottery was produced.

Furthermore, this study shows the potential of micromor-phology to resolve debated issues concerning the contextual integrity of objects within cultural deposits, especially bones and charcoal that are used as dating samples. Our results lend further support to the validity of the dating of Xianrendong early pottery (Wu et al.2012; Cohen et al.2017), as we show that bioturbation at any given time at Xianrendong is very weak. This supports the inference that the radiocarbon-dated materials are contemporary with the stratum of their original deposition and were not moved post-depositionally.

Xianrendong and other caves in South China, such as Yuchanyan in Hunan (Boaretto et al. 2009), show hunter-gatherers producing pottery from 20,000 calBPonward, some

10,000 years before the first sedentary settlements appear along with the onset of agricultural activities. The specific roles of the caves within hunter-gatherer societies from the LGM through the Terminal Pleistocene, however, remain poorly understood. The micromorphological study here is a first step in gaining such understanding. At Xianrendong, fur-ther investigation is needed to support our hypothesis that human activities centered outside the entrance of the cave while within the cave vestibule itself, human behaviors are primarily associated with dumping and not directly with do-mestic activities such living areas, food preparation and cooking, bone and stone tool and pottery manufacture, or other daily-life activities.

To fully understand human behavior in South China at the time when Upper Paleolithic hunter-gatherers first invented pottery, it is necessary to apply geoarchaeological techniques consistently across the complete set of sites. This must be done in combination with other scientific methods of investi-gation, as questions of site function, formation processes, and dating remain poorly understood. Such studies should provide better insights into hunter-gatherer adaptations and

ƒ

Fig. 18 Time–depth plots illustrating depositional rates. a The WP shows

a depositional hiatus between ~ 27,000 and 21,000 calBP, followed by periods of regular input of alluvium. b The EP, in contrast, shows moments of relatively rapid sedimentation. Between ~ 25,000 and 20,000 calBP, we see the appearance of anthropogenic sediments in the east along with some roof fall that increase the volume of the sediments. Relatively slow deposition in the west between ~ 20,000 and 14,000 cal

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activities—including subsistence and ritual behaviors—and in particular into the reasons for the invention of pottery in the context of foraging economies.

Acknowledgments Funding for this project was provided through grants from the National Science Foundation (USA) (no. 0917739 and no. 0551927) and the American School for Prehistoric Research (Peabody Museum, Harvard University). Logistical support was provided by the Jiangxi Provincial Government, Wannian County Government, and Jiangxi Provincial Museum, and we extend our gratitude for their gra-cious and enthusiastic help.

Publisher’s note Springer Nature remains neutral with regard to jurisdic-tional claims in published maps and institujurisdic-tional affiliations.

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