• 沒有找到結果。

以 3 omega 方法量測薄膜之賽貝克因子

第五章 總結與未來工作

5.2 未來工作

5.2.2 以 3 omega 方法量測薄膜之賽貝克因子

probe(圖 5.2 中紅色部分,圖中之黃色為 contact pad)介於此超晶格薄膜與金 屬層間,其與另一個於基材底部之 voltage probe 一起用以量測垂直方向穿

準確得知熱電材料垂直平面方向的ZT值。

圖 5.2 量測賽貝克因子之系統示意圖[44]

1w heat source

Substrate

TE film V2w

insulator insulator voltage probe

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附錄 A:誤差分析

頻率為 995.5Hz 之 V3ω值來進行分析,各參數如表 A.1 所示。 Digital Multimeter)量測阻值之量測誤差(該儀器之精準度為 0.01%,測得外 接電阻值為 34.0942Ω)所造成;所使用的電阻其溫度係數為 20ppm/K,假設 量測過程中室內溫度變化為 0.5K,則室內溫度變化所造成之誤差為 0.001%,

因此

R

out 約為 0.01%,因此將上述資料搭配表 A.1 代入式(A.7)分別求得

待測樣品與參考樣品之加熱線電阻的誤差 0

附錄 B:量測數據

在 4.1 節實驗數據分析技巧當中,已附上厚度為 680nm sample1(圖 4.2)之實 驗量測數據之

V

對頻率作圖,以下為其餘八組實驗數據之

V

訊號對頻率 作圖,其中實心的方塊為待測元件的

V

3ω,total訊號,空心方塊為參考元件的

3ω,sub

V

訊號。量測溫度標於圖的右上角。

厚度 280 nm sample1(計算時,所取頻率範圍為 100-1000Hz):

圖 B.1 厚度 280 nm 之碲化鉛薄膜 sample1 量測數據

厚度 280 nm sample2(計算時,所取頻率範圍為 100-2000Hz):

圖 B.2 厚度 280 nm 之碲化鉛薄膜 sample2 量測數據

厚度 280 nm sample3(計算時,所取頻率範圍為 100-2000Hz):

圖 B.3 厚度 280 nm 之碲化鉛薄膜 sample3 量測數據

厚度 460 nm sample1(計算時,所取頻率範圍為 200-2000Hz):

圖 B.4 厚度 460 nm 之碲化鉛薄膜 sample1 量測數據

厚度 460 nm sample2(計算時,所取頻率範圍為 200-2000Hz):

圖 B.5 厚度 460 nm 之碲化鉛薄膜 sample2 量測數據

厚度 460 nm sample3(計算時,所取頻率範圍為 200-2000Hz):

圖 B.6 厚度 460 nm 之碲化鉛薄膜 sample3 量測數據

厚度 680 nm sample2(計算時,所取頻率範圍為 100-1000Hz):

圖 B.7 厚度 680 nm 之碲化鉛薄膜 sample2 量測數據

厚度 680 nm sample3(計算時,所取頻率範圍為 100-1000Hz) :

圖 B.8 厚度 680 nm 之碲化鉛薄膜 sample3 量測數據

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