135
第一部分
10987654321ppm 1.00 2.11 1.10 2.06 2.09 2.09 2.08 2.04 Current Data Parameters NAME DH190 EXPNO 25 PROCNO 1 F2 - Acquisition Parameters Date_ 20170704 Time 17.57 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 228.1 DW 69.000 usec DE 6.50 usec TE 297.1 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 16.80 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300078 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
136
137
10987654321ppm 1.00 2.10 3.12 4.13 2.11 2.06 Current Data Parameters NAME DH134 EXPNO 25 PROCNO 1 F2 - Acquisition Parameters Date_ 20170704 Time 0.47 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 322.5 DW 69.000 usec DE 6.50 usec TE 296.7 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 16.80 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300091 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
138
139
10987654321ppm 1.00 2.11 1.10 4.23 2.10 2.10 2.09 Current Data Parameters NAME DH291 EXPNO 8 PROCNO 1 F2 - Acquisition Parameters Date_ 20170622 Time 18.14 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 181 DW 69.000 usec DE 6.50 usec TE 298.5 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 16.80 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300105 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
140
141
10987654321ppm 3.07
1.00 2.03 4.04 2.03 2.05 2.02 Current Data Parameters NAME DH310 EXPNO 15 PROCNO 1 F2 - Acquisition Parameters Date_ 20170627 Time 22.27 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 181 DW 69.000 usec DE 6.50 usec TE 296.9 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 16.80 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300096 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
142
143
10987654321ppm
1.00 2.06 2.12 2.07 2.04 2.12 2.05 Current Data Parameters NAME DH313 EXPNO 13 PROCNO 1 F2 - Acquisition Parameters Date_ 20170629 Time 23.09 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 256 DW 69.000 usec DE 6.50 usec TE 297.6 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 16.80 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300096 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
144
145
第二部分
10987654321ppm 2.09 2.07
1.00 4.01 6.03 7.03 1.06 1.00 2.01 Current Data Parameters NAME KL347 EXPNO 2 PROCNO 1 F2 - Acquisition Parameters Date_ 20160322 Time 11.58 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 228.1 DW 69.000 usec DE 6.50 usec TE 296.6 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300109 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
146
147
10987654321ppm 2.20 2.20 3.02
1.00 2.02 4.05 6.08 4.93 1.00 2.02 Current Data Parameters NAME KL346 EXPNO 3 PROCNO 1 F2 - Acquisition Parameters Date_ 20160515 Time 14.28 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 322.5 DW 69.000 usec DE 6.50 usec TE 299.5 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300118 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
148
149
10987654321ppm 2.04 2.10
1.00 4.06 6.08 7.19 0.99 2.03 Current Data Parameters NAME DH126 EXPNO 20 PROCNO 1 F2 - Acquisition Parameters Date_ 20170425 Time 10.43 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 181 DW 69.000 usec DE 6.50 usec TE 295.1 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300122 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
150
151
10987654321ppm 2.16 2.13
1.00 4.07 6.09 5.20 1.01 2.02 2.02 Current Data Parameters NAME DH114 EXPNO 23 PROCNO 1 F2 - Acquisition Parameters Date_ 20170425 Time 20.34 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 256 DW 69.000 usec DE 6.50 usec TE 297.8 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300109 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
152
153
10987654321ppm 1.90 2.00
1.00 4.01 6.04 7.29 1.03 2.02 Current Data Parameters NAME TOM-024 EXPNO 1 PROCNO 1 F2 - Acquisition Parameters Date_ 20170301 Time 15.19 INSTRUM spect PROBHD 5 mm PABBO BB/ PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 32 DS 0 SWH 7211.539 Hz FIDRES 0.220079 Hz AQ 2.2719147 sec RG 78.51 DW 69.333 usec DE 10.50 usec TE 297.3 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== SFO1 400.1324008 MHz NUC1 1H P1 12.90 usec PLW1 15.00000000 W F2 - Processing parameters SI 16384 SF 400.1300153 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
154
155
10987654321ppm 4.02
1.00 2.06 5.21 6.20 3.38 2.10 1.05 Current Data Parameters NAME TOM-067 EXPNO 2 PROCNO 1 F2 - Acquisition Parameters Date_ 20170303 Time 18.03 INSTRUM spect PROBHD 5 mm PABBO BB/ PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 1 DS 0 SWH 7211.539 Hz FIDRES 0.220079 Hz AQ 2.2719147 sec RG 24.54 DW 69.333 usec DE 10.50 usec TE 298.4 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== SFO1 400.1324008 MHz NUC1 1H P1 12.90 usec PLW1 15.00000000 W F2 - Processing parameters SI 16384 SF 400.1300387 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
156
157
10987654321ppm 2.04 2.02
1.00 4.01 2.15 5.86 2.14 2.07 1.00 1.04 2.02 Current Data Parameters NAME DH047 EXPNO 1 PROCNO 1 F2 - Acquisition Parameters Date_ 20160411 Time 17.07 INSTRUM spect PROBHD 5 mm PABBO BB/ PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7211.539 Hz FIDRES 0.220079 Hz AQ 2.2719147 sec RG 89.08 DW 69.333 usec DE 10.50 usec TE 297.7 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== SFO1 400.1324008 MHz NUC1 1H P1 12.90 usec PLW1 15.00000000 W F2 - Processing parameters SI 16384 SF 400.1300000 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
158
159
10987654321ppm 2.06 2.06
1.00 4.07 8.18 3.12 2.05 1.09 2.02 Current Data Parameters NAME Tom035 EXPNO 7 PROCNO 1 F2 - Acquisition Parameters Date_ 20161221 Time 15.19 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 114 DW 69.000 usec DE 6.50 usec TE 295.2 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300114 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
160
161
10987654321ppm 2.01 2.04
1.00 1.04 4.08 0.89 1.08 6.14 2.11 1.02 0.98 2.08 0.98 Current Data Parameters NAME Tom055 EXPNO 11 PROCNO 1 F2 - Acquisition Parameters Date_ 20161213 Time 12.24 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 114 DW 69.000 usec DE 6.50 usec TE 295.7 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300145 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
162
163
10987654321ppm 2.04 2.06 3.07
1.00 2.05 4.10 6.15 2.04 2.06 1.07 1.02 2.06 Current Data Parameters NAME DH098 EXPNO 1 PROCNO 1 F2 - Acquisition Parameters Date_ 20161221 Time 2.31 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 181 DW 69.000 usec DE 6.50 usec TE 296.3 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300118 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
164
165
10987654321ppm 4.13
0.99 1.00 0.99 4.09 6.10 3.04 2.00 2.01 Current Data Parameters NAME DH118 EXPNO 3 PROCNO 1 F2 - Acquisition Parameters Date_ 20160421 Time 17.20 INSTRUM spect PROBHD 5 mm PABBO BB/ PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7211.539 Hz FIDRES 0.220079 Hz AQ 2.2719147 sec RG 99.72 DW 69.333 usec DE 10.50 usec TE 298.1 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== SFO1 400.1324008 MHz NUC1 1H P1 12.90 usec PLW1 15.00000000 W F2 - Processing parameters SI 16384 SF 400.1300131 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
166
167
10987654321ppm 1.85 2.16
1.00 2.23 3.72 9.73 1.97 2.15 1.05 1.06 4.09 Current Data Parameters NAME DH129 EXPNO 6 PROCNO 1 F2 - Acquisition Parameters Date_ 20160512 Time 12.06 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 114 DW 69.000 usec DE 6.50 usec TE 297.4 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300140 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
168
169
10987654321ppm 1.93 2.25 3.10
1.00 2.14 2.28 3.61 8.27 0.86 2.08 1.05 4.08 Current Data Parameters NAME Tom088 EXPNO 58 PROCNO 1 F2 - Acquisition Parameters Date_ 20170525 Time 17.55 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 161.3 DW 69.000 usec DE 6.50 usec TE 299.0 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300131 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
170
171
10987654321ppm 2.03 2.16
1.00
6.14 8.22 1.27 2.22 2.07 1.04 2.00 2.03 Current Data Parameters NAME DH128 EXPNO 12 PROCNO 1 F2 - Acquisition Parameters Date_ 20160418 Time 18.01 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 114 DW 69.000 usec DE 6.50 usec TE 296.8 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300122 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
172
173
10987654321ppm 2.00 2.07
1.00 3.09 2.61 8.12 0.79 2.08 1.06 2.01 2.05 2.02 Current Data Parameters NAME Tom078 EXPNO 19 PROCNO 1 F2 - Acquisition Parameters Date_ 20170521 Time 12.08 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 35.9 DW 69.000 usec DE 6.50 usec TE 295.3 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300264 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
174
175
10987654321ppm 1.92 2.06
1.00
6.00 9.01 0.95 2.05 2.06 1.04 1.98 2.03 Current Data Parameters NAME Tom079 EXPNO 15 PROCNO 1 F2 - Acquisition Parameters Date_ 20170518 Time 17.02 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 10 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 35.9 DW 69.000 usec DE 6.50 usec TE 295.2 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300286 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
176
177
10987654321ppm 2.09 2.09
1.01 1.00 5.22 8.16 2.70 1.13 1.94 1.02 1.03 1.99 Current Data Parameters NAME Tom122 EXPNO 88 PROCNO 1 F2 - Acquisition Parameters Date_ 20170525 Time 14.27 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 79 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 114 DW 69.000 usec DE 6.50 usec TE 300.2 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300141 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
178
179
10987654321ppm 1.96 2.09
1.00 2.03 3.97 5.97 2.04 1.97 2.08 1.06 1.03 4.05 Current Data Parameters NAME DH119 EXPNO 9 PROCNO 1 F2 - Acquisition Parameters Date_ 20160510 Time 17.58 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 114 DW 69.000 usec DE 6.50 usec TE 298.2 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300149 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
180
181
10987654321ppm 2.14 2.26
1.00 1.13 1.10 2.10 3.08 7.08 1.12 2.38 1.83 1.18 1.14 4.29 Current Data Parameters NAME DH234 EXPNO 33 PROCNO 1 F2 - Acquisition Parameters Date_ 20170519 Time 21.45 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 57 DW 69.000 usec DE 6.50 usec TE 295.1 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300185 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
182
183
10987654321ppm 4.23
0.99 1.01 1.00 4.16 6.23 3.07 2.06 1.06 1.05 2.06 2.05 Current Data Parameters NAME TOM-124 EXPNO 3 PROCNO 1 F2 - Acquisition Parameters Date_ 20170323 Time 13.57 INSTRUM spect PROBHD 5 mm PABBO BB/ PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 32 DS 0 SWH 7211.539 Hz FIDRES 0.220079 Hz AQ 2.2719147 sec RG 78.51 DW 69.333 usec DE 10.50 usec TE 297.7 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== SFO1 400.1324008 MHz NUC1 1H P1 12.90 usec PLW1 15.00000000 W F2 - Processing parameters SI 16384 SF 400.1300140 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
184
185
10987654321ppm 1.92 2.09
1.00
2.05 3.80 6.03 2.08 4.07 1.03 2.03 2.03 Current Data Parameters NAME Tom014 EXPNO 21 PROCNO 1 F2 - Acquisition Parameters Date_ 20170324 Time 10.51 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 17 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 114 DW 69.000 usec DE 6.50 usec TE 298.3 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300140 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
186
187
10987654321ppm 1.00 1.03 2.07 3.02
1.00 2.08 3.02 3.08 6.05 2.18 2.12 1.04 1.98 2.03 Current Data Parameters NAME Tom032 EXPNO 3 PROCNO 1 F2 - Acquisition Parameters Date_ 20161116 Time 17.53 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 16 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 114 DW 69.000 usec DE 6.50 usec TE 295.4 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300118 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
188
189
10987654321ppm 2.00 2.23
1.02
2.09 4.13 6.05 2.14 2.14 1.10 2.08 2.06 2.05 Current Data Parameters NAME Tom033 EXPNO 13 PROCNO 1 F2 - Acquisition Parameters Date_ 20170407 Time 13.37 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 32 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 114 DW 69.000 usec DE 6.50 usec TE 297.9 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300118 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
190
191
10987654321ppm 2.01 2.07
1.00
2.02 4.07 6.06 2.15 0.93 2.16 2.97 1.02 2.03 Current Data Parameters NAME Tom060 EXPNO 16 PROCNO 1 F2 - Acquisition Parameters Date_ 20170408 Time 16.27 INSTRUM spect PROBHD 5 mm BBO BB-1H PULPROG zg30 TD 32768 SOLVENT CDCl3 NS 13 DS 0 SWH 7246.377 Hz FIDRES 0.221142 Hz AQ 2.2609921 sec RG 114 DW 69.000 usec DE 6.50 usec TE 298.8 K D1 2.00000000 sec TD0 1 ======== CHANNEL f1 ======== NUC1 1H P1 14.40 usec PL1 1.80 dB SFO1 400.1324008 MHz F2 - Processing parameters SI 16384 SF 400.1300146 MHz WDW EM SSB 0 LB 0 Hz GB 0 PC 1.00
192