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Cell migration plays an important role in physiology and disease (Gardel,

Schneider et al. 2010). Cells fail to migrate to the right position during embryogenesis

may cause severe development disorders. Cancer cells might change the extra cellular

matrix (ECM) and induce a series of events to help them migrate to other organs, the

metastasis. For tissue engineering, constructing an appropriate microenvironment and

guiding the cells to the right place are critical for cells to function as they did in the

original organs. Therefore, understanding the fundamental mechanisms of cell

migration is crucial to create strategies for disease treatment and regenerative

medicine.

Biochemical and biomechanical cues are two major stimulation types to guide

cell migration, and clarifying how these signals affect cell migration is an important

research field. Microfluidic systems are capable to generate stable linear or

logarithmic chemical gradients and therefore are widely used to study chemotaxis,

which describe how chemical factors attract or repel cell migrate along the direction

of chemical gradient. Human neutrophils migrate to the place with the highest

concentration of interleukin-8 (IL-8) and demonstrate different behaviors to different

gradient patterns (Li Jeon, Baskaran et al. 2002). Venular and arterial endothelial cells

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show different reactions to the gradient of fibroblast growth factor 2 (FGF2) and

different gradient strengths of vascular endothelial growth factor A 165 (VEGFA165)

could induce human umbilical vein endothelial cells (HUVECs) to generate different

chemotaxis responses (Barkefors, Le Jan et al. 2008).

Astrocyte has been observed to migrate toward hypotonic region under an

osmotic gradient (Saadoun, Papadopoulos et al. 2005), and that observation might be

involved with the water flow through aquaporins (AQPs) on the cell membrane

(Papadopoulos, Saadoun et al. 2008) Some other experiments also show that the

osmolarity play a role in controlling cell motility (Loitto, Karlsson et al. 2009). A

theoretical study proposes that the osmotic gradient can induce water flux to facilitate

the cell motility (Jaeger, Carin et al. 1999). Although the mechanism is still not clear,

the osmotic gradient might be a fundamental mechanical stimulation to guide cell

migration.

Substrate stiffness is another important mechanical stimulation that has been

shown to control the differentiation of mesenchymal stem cells (Engler, Sen et al.

2006) and cell migration. 3T3 fibroblast (Lo, Wang et al. 2000), vascular smooth

muscle cells (Wong, Velasco et al. 2003; Isenberg, DiMilla et al. 2009) and

macrophages (Nemir, Hayenga et al. 2010) have been demonstrated that they would

migrate to stiffer region from softer region of the substrata. This phenomenon is

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durotaxis, and the most common material to study how cell response to substrata

biophysical signals is polyacrylamide (PA) gel (Gribova, Crouzier et al. 2011). The

preparation and characteristics of polyacrylamide gel are well established and studied

(Tse and Engler 2010).

Although these studies have shown deep insights to explain the relation between

one specific signal and cell migration, there are still few have built an environment

providing dual or multiple gradient cues simultaneously. Understanding the cell

behaviors under a more in vivo-like situation will further extend our knowledge to cell

migration and have more reliable information for medical application. However, this

idea is mainly limited by the nature that one method can usually generate only one

well-controlled signal. One of the approaches to overcome this challenge with

microfluidics is designing a functional channel-geometry to generate shear stress

gradients in one cell culture chamber, thus it can cooperate with chemical gradient to

guide cell migration at the same time (Park, Yoo et al. 2009). Despite their many

benefits, there are a number of small, but important, problems. For example, the two

stimulations could not be controlled independently since the chemical gradient is also

influenced by the flow profile. Another weakness is that the real flow velocity is very

difficult to be measured for the flow direction is not simply straight. Moreover, the

properties of substrata still could not be changed while these signals are also critical to

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guide cell migration.

In this study, we propose a new approach that integrates two different systems

into a dual cues device which can generate substrate stiffness and osmotic gradients

simultaneously. The two systems in this device are: (1) a gradient-compliant PA gel

which is responsible for the first mechanical cue, the substrate stiffness gradient, and

(2) a microfluidic system which can generate the second mechanical cue, the osmotic

gradient. Sucrose is selected here to adjust the osmolarity of the cell culture media,

and it has been used before to study the effect of hypertonic stress on C2C12 cells

(Alfieri, Bonelli et al. 2006). The design of the microfluidic system can be divided

into two sides: (1) the source side which continues to provide cell culture media with

highest sucrose concentration to the cell culture chamber in the microfluidics, and (2)

the free side which allows the cell culture chamber to access the bulk solution without

sucrose. The gradient is built through the diffusion of sucrose from source side to free

side and can be maintained for long term cell culture studies. To develop our dual

cues device, we have created two new steps to embed the PA gel in the microfluidic

system and protect the gel from damages during the conventional

poly(dimethylsiloxane) (PDMS) microfluidics fabrication process.

The C2C12 mouse myoblast is an appropriate candidate to be investigated with

osmotic and stiffness gradients. This cell line has been shown that the expression of

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AOP5 is regulated by differentiation and hypertonic stress (Hwang, Lee et al. 2002).

The morphology of C2C12 cells is found to depend on substrate stiffness (Engler,

Griffin et al. 2004). However, the effects of these mechanical cues on C2C12 cell

migration are still not clear.

We hypothesize that C2C12 cell migration can be influenced by both stiffness

and osmotic gradients and the two signals can facilitate with each other to guide cell

migration. So far, we have successfully performed C2C12 cell culture in our device.

We also cultured C2C12 cells with a high osmolarity cell culture medium in the

culture dish, and analyzed cell migration on a gradient-compliant PA gel. These

results provide important information for further experiments to test our hypotheses.

The device presented in this study might be the first one to embed a

gradient-compliant PA gel in a microfluidic system, and this device has the potential

to be used to study cell migration under two different stimulations which is more

close to the in vivo system. The first stimulation is stiffness gradient, and the second

one can be osmotic gradients or theoretically, chemical gradients if the solute is

replaced with chemoacttractants, thus making the device more flexible to be adopted

for other studies.

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