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CHAPTER 2 MATHEMATICAL MODELING

2.5 Numerical Procedures

2.5.3 Model Validation

In the simulation, a uniform grids distribution is used to calculate the complex

electrochemical reaction and physical phenomena in the fuel cell. Three mesh

systems- 41 x 13 x 47, 51 x 16 x 58, and 61 x 21 x 67 are constructed to explore

numerical result dependence on computational cell numbers. Table 2.1 presents

geometrical and operating parameters of the base model in the PEM fuel cell. The

results of the polarization curve by the base model under different grid systems are

shown in Fig. 2.3. Considering both accuracy and economics, the grid system of 51 in

the z-direction, 16 in the x-direction, and 58 in the y-direction was selected for present

research.

To further check the adequacy of the numerical scheme, it is clearly seen from

Fig. 2.4 that the present predictions agree reasonably with the experimental data of

Squadrito et al. [44]. The above preliminary runs confirm that the present model and

the numerical method used are generally appropriate in analysis of the present

problem.

3 [14]

Tortuosity of the diffusion and catalyst layers

0.5 / 1.5 [14] Relative humidity of anode/cathode inlet

1.5 / 3 [44]

Stoichiometry, at / at 1.0

0.28 [45]

Porosity of membrane

0.4 / 0.4 [45]

Porosity of diffusion and catalyst layers

[14]

Permeability of membrane

/ [14]

Permeability of diffusion and catalyst layers

3 [14]

Tortuosity of the diffusion and catalyst layers

0.5 / 1.5 [14] Relative humidity of anode/cathode inlet

1.5 / 3 [44]

Stoichiometry, at / at 1.0

0.28 [45]

Porosity of membrane

0.4 / 0.4 [45]

Porosity of diffusion and catalyst layers

[14]

Permeability of membrane

/ [14]

Permeability of diffusion and catalyst layers

Table 2.1. Geometrical and operating parameters

Quantity Value

Cathode BP Anode BP

Cathode Channel

Anode Channel

Cathode GDL Cathode CL

Membrane Anode CL Anode GDL

X Y

Z

Cathode BP Anode BP

Cathode Channel

Anode Channel

Cathode GDL Cathode CL

Membrane Anode CL Anode GDL

X Y

Z

Figure 2.1 Physical and computational domains considered in this study

Begin

Solve momentum eq. obtain u*, v*, w*

Obtain pressure and velocity correction Guess P*

Set P*=P Stop

Solve for scalar equations of species, enthalpy, potential field Obtain mass imbalances

Correct pressure and velocity fields

Converged ?

Solve momentum eq. obtain u*, v*, w*

Obtain pressure and velocity correction Guess P*

Set P*=P Stop

Stop

Solve for scalar equations of species, enthalpy, potential field Obtain mass imbalances

Correct pressure and velocity fields

Converged ?

Figure 2.2 Numerical flow diagram of the solution procedure.

0 0.2 0.4 0.6 0.8 1 1.2

0 0.2 0.4 0.6 0.8 1 1.2

41 x 13 x 47 51 x 16 x 58 61 x 21 x 67

Vo lt a g e ( V )

Current Density ( A/cm

2

)

Figure 2.3 Comparison of predictions on the three different grid systems.

0.3 0.4 0.5 0.6 0.7 0.8 0.9 1

0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8

Squadrito et al. [44]

Present result

Vo lt a ge ( V )

Current Density ( A/cm

2

)

Figure 2.4 Comparison of the predicted I–V curve and the experimental data of Squadrito et al. [44].

CHAPTER 3

EFFECTS OF CATHODE HUMIDIFICATION AND POROSITY OF THE GDL ON THE GAS–LIQUID INTERFACE LOCATION IN A PEM FUEL CELL

3.1 Introduction

A PEM fuel cell is prone to gas-liquid two-phase formation due to its low

operating temperature, particularly under highly humidified or high current density

conditions. When the gas diffusion layer and the catalyst layer become saturated with

water vapor, the product water starts to condense and block open pores, reducing the

available paths for oxygen transport. This phenomenon is termed “flooding” and

becomes a major limiting factor of PEM fuel cell performance. Hence, it is critical to

understand the two-phase flow and transport in a PEM fuel cell, and a mathematical

model is useful to improve this understanding. In practice, humidification of anode

fuels and/or cathode oxidants is often used to provide sufficient membrane hydration.

Since water is generated in the cathode catalyst layer from electrochemical reaction

and it also tends to migrate from the anode side to the cathode side by the

electro-osmotic drag, it becomes a key issue in the design and operation of PEM fuel

cells to avoid the flooding phenomenon in the cathode. In this chapter, effects of

cathode humidification and gas diffusion layer porosity on the gas-liquid interface

location in a PEM fuel cell are investigated and described in detail. For all of the

calculations carried out in this study, the fuel flows were co-flows and inlet

stoichiometric ratios of 1.5 and 3 are used for the anode and cathode sides based on a

reference current density of 1 A/cm2. The inlet fuel, hydrogen, is assumed to be fully

humidified on the anode-side; the cell temperature and humidification temperature are

343 K and the operating pressure is 1 atm.

3.2 Effects of cathode humidification scheme

In this study, the location of the gas-liquid interface along the flow channel

direction at various cathode humidity conditions and its effect on cell performance are

elucidated by modeling a three-dimensional PEM fuel cell system using CFD. Figure

3.1 shows the effect of the relative humidity of the cathode on the location of the

interface where the liquid water begins to condense along flow channel at a cell

operating voltage of 0.7 V. The interface is defined as the location where liquid water

begins to condense. The horizontal dotted line indicates the interface between the flow

channel and the gas diffusion layer. A higher cathode relative humidity corresponds to

a smaller distance between the gas-liquid interface and the gas inlet, as clearly

displayed in Fig. 3.1 (a). Furthermore, the gas-liquid interface location moves to the

flow channel inlet region as the relative humidity of the cathode increases. This

phenomenon is caused by: (i) the decrease in the amount of evaporated water through

the flowing gas stream; (ii) the increase in the partial pressure of water and the ability

to reach the saturation pressure of the vapor water relatively quickly to form liquid

water earlier as the relative humidity of the cathode increases. On the contrary, the

gas-liquid interface location moves closer to the cathode catalyst layer when the

relative humidity of the cathode is less than 60%, as shown in Fig. 3.1 (b). In

conclusion, increasing the relative humidity of the cathode can reposition the

gas-liquid interface and cause liquid water to appear, affecting the performance of the

cell, because liquid water may occupy the pores in the porous media, reducing the

amount of fuel gas that can reach the cathode catalyst layer. Figures 3.2 (a) and 3.2 (b)

plot I–V and I–P curves at various relative humidity of the cathode with conventional

flow fields. The results in Fig. 3.2 (a) reveal that the cell performance decreases as the

relative humidity of the cathode increases, because the amount of liquid water

increases with the relative humidity. Accordingly, the pores in the porous media were

obstructed by liquid water at the cathode-side, reducing the amount of reaction gas to

the cathode catalyst layer. Therefore, the performance of the cell gradually decreases.

Also, the polarization curves do not seem to vary as the relative humidity of the

cathode increases, at an operating voltage that exceeds ~0.65 V. A large voltage results

in a small current density, and therefore, a relatively small electrochemistry reaction

rate. However, the performance of the cell decreases significantly as the operating

voltage declines below the ~0.65 V operating voltage, since the large current density

accelerates the rate of the electrochemical reaction. In particularly, in Fig. 3.2 (a), the

higher cathode relative humidity (100%) offers a better cell performance than the

lower one (20%) at an operating voltage of over ~0.65 V, because the rate of the

electrochemical reaction decreases as the operating voltage increases. Therefore, the

water content of the membrane in the initial stage increases with the relative humidity.

Thus, the cell performance is improved as the relative humidity of the cathode

increases.

By contrast, at operating voltages of below ~0.65 V, the cell performance

improves as the relative humidity of the cathode decreases, because accelerating the

electrochemical reaction produces more water, increasing the water content in the

membrane at a low cathode relative humidity, such as 20%. However, at high relative

humidity, flooding may occur at the cathode-side. Additionally, the power density

increases as the relative humidity of the cathode decreases, as shown in Fig. 3.2 (b).

3.3 Effects of cell operating voltage

Figure 3.3 shows the effects of various operating voltages on the location of

the gas-liquid interface along the flow channel at a relative humidity of the cathode of

80%. Figure 3.3 reveals that the gas-liquid interface location is close to the cathode

catalyst layer at high operating voltage, indicating that less water was generated at a

lower electrochemical reaction rate. However, since more water is generated at a high

electrochemical reaction rate, the gas-liquid interface location is close to the gas

diffusion layer and the flow channel at a low operating voltage. In closing, the

gas-liquid interface location gradually moves to the gas channel inlet region as the

operating voltage decreases, because reducing the operating voltage increases the

current density. Therefore, the electrochemical reaction rate increases.

3.4 Three-dimensional species field

Figures 3.4 and 3.5 plot the oxygen and water fractions in the gas flow channel

and the gas diffusion layer, respectively, of the cathode-side in the direction of the

flow channel at an operating voltage of 0.7 V and relative humidity of the cathode at

80%. Larger oxygen fraction appears in the gas channel inlet region, and then

gradually decreases in the flow channel direction, as shown in Fig. 3.4. The results

reveal that the decrease in the oxygen fraction is caused by the catalyst layer

consuming more oxygen on the cathode-side. Hence, the oxygen fraction is lowest

near the cathode catalyst layer. By contrast, Fig. 3.5 reveals that the water fraction

gradually increases along the flow channel direction, because of the production of

water in the catalyst layer of the cathode by the electrochemical reaction, as well as

the transport of water from the anode-side to the cathode-side by electro-osmotic drag.

Accordingly, the water fraction is the highest near the cathode catalyst layer. Since the

water mass fraction is higher near the cathode catalyst layer, where the corresponding

water partial pressure exceeds the saturated vapor pressure, causing the formation of

liquid water. Therefore, Fig. 3.6 shows the liquid water saturation field in the gas

channel and the gas diffusion layer of the cathode-side at an operating voltage of 0.7

V and a relative humidity of the cathode of 80%. The figure shows that saturation of

the liquid water increases along the flow channel direction, because the

electrochemical reaction causes the partial pressure of the water to exceed the

saturated vapor pressure, causing liquid water to condense. The capillary force also

causes liquid water to move toward the gas diffusion layer. Hence, this interface is the

single-phase region when the saturation of the liquid water is zero. It becomes a

two-phase region when the saturation of the liquid water exceeds zero. According to

Fig. 3.1, to the right of the point where water condensation starts, a two-phase region

is present along the flow channel direction. A single-phase region exists on the other

side.

Figures 3.7 show that the oxygen mass fraction contours at the cathode gas

diffusion layer as the cathode humidification of (a) 20% (b) 60% (c) 100% for cell

voltage of 0.4 V. It is obvious from these plots that the oxygen mass fraction gradually

decreased along the flow channel direction from the inlet toward outlet owing to the

consumption of oxygen by the electrochemical reaction in the cathode catalyst layer.

This figure also shows that the oxygen mass fraction decreases as the cathode

humidification increases from the 20% to 100%. This is attributed to the fact that a

higher relative humidity of cathode causes greater amount of water vapor enters the

electrode; therefore more liquid water is apt to condense in the pore space. Hence, the

amount of the oxygen through the gas diffusion layer is reduced and the cell

performance is decreased. Figures 3.8 presents the mass fraction contours of water

vapor at the cathode gas diffusion layer as the cathode humidification of (a) 20% (b)

60% (c) 100% for cell voltage of 0.4 V. The results reveal the fact that water fraction

gradually increases along the flow channel direction owning to the production of

water in the cathode catalyst layer by the electrochemical reaction. Also the water

concentration increases in the gas diffusion layer as the cathode humidification

increases. The distributions of the liquid water saturation for these cases are showed

in Fig 3.9. From these figures, it is found that when the cathode humidification is 20%,

the amount of the liquid water in the gas diffusion layer is almost very small.

However, when the cathode humidification is 100%, the there is some liquid water

appears in the gas diffusion layer. Hence, the pores in the gas diffusion layer were

obstructed by liquid water, reducing the amount of oxygen to the cathode catalyst

layer. Therefore, it supports the argument of previous plot, namely, the oxygen mass

fraction decreased owing to the blocking of liquid water in the pore of the porous

media as the cathode humidification increases.

3.5 Two-phase mixture velocity field

Figure 3.10 shows the velocity field of the two-phase mixture in the gas

diffusion layer and flow channel of the cathode at the cell voltage of 0.7 V and

cathode relative humidity of 80%. As expected, there is a large difference in the

velocity scale between the gas diffusion layer and the flow channel. The mixture

velocity in the gas diffusion layer is at least two orders of magnitude smaller than that

in the flow channel, indicating that gas diffusion is the dominant transport mechanism

in the porous media. The flow field in the flow channel is fully developed in view of

the large aspect ratio of the channel length to height (equal to 93 in the present study),

as can be seen from Fig. 3.7 where the channel length is, however, not drawn to scale

for better view.

3.6 Effects of the cathode gas diffusion layer porosity

The porosity of the cathode gas diffusion layer has two different effects on the

fuel cell performance: as the porous region provides the space for the reactants to

diffuse towards the catalyst layer region, an increase in the porosity means that the

onset of mass transport limitations occurs at higher current densities, i.e. it leads to

higher limiting currents. The adverse effect of a high porosity is an expected increase

in the contact resistance. Contact resistance occurs at all interfaces inside the fuel cell,

the most important one being the interface between the bipolar plates and the gas

diffusion layers. In this study, the solid phase conductivity is assumed constant and

does not change with the variation of GDL porosity. Hence, the location of the

gas-liquid interface along the flow channel direction at various porosities of the

cathode gas diffusion layer and its effect on cell performance were elucidated. Figure

3.11 shows the effects of the cathode gas diffusion layer porosity on the location of

the gas-liquid interface where the liquid water begins to condense along flow channel

direction at a cell voltage of 0.7 V and a relative humidity of the cathode of 80%. The

results in Fig. 3.11 show that the location of the gas-liquid interface appears early and

is closed to the flow channel inlet region in the gas diffusion layer as the gas diffusion

layer porosities decreased. These phenomena can be explained as that given smaller

porosity of the gas diffusion layer, the liquid water is more difficult to transport out of

the gas diffusion layer, hence, the liquid water will spread throughout the gas

diffusion layer. Once the liquid water block the pores of the porous media, causing the

hinder the diffusion transport of fuel gas to the cathode catalyst layer, thus limiting the

electrochemical reaction and causeing the decrease of cell performance. On the

contrary, the higher porosity of the cathode gas diffusion layer facilitates the transport

of water from the cathode catalyst layer to the flow channel. Hence, less water blocks

the pores of the gas diffusion layer, increasing the vacant pores space and helping the

reactant diffusion to the cathode catalyst layer. Nevertheless, the variation of the

gas-liquid interface location becomes small as the porosity changes from 0.7 to 0.8.

The phenomenon can be conjectured as that when the cathode gas diffusion layer

porosity is too big, the capillarity effect is not sensible, hence, the gas-liquid interface

location doesn’t seem to change obviously.

Figures 3.12 (a) and 3.12 (b) show I-V and I-P curves at various porosities of

the cathode gas diffusion layer at a relative cathode humidity of 80%. In Fig. 3.12 (a)

the I–V curves demonstrate that a better performance can be obtained by using a gas

diffusion layer of higher porosity. The remarkable drop in cell potential is caused by a

mass transfer or concentration loss, which is a consequence of shortage of the reactant

gas at high current density in which more reactant gas is required for fast reaction. A

gas diffusion layer of higher porosity has an ability of stronger diffusion transport,

which is beneficial in that it supplements the reactant gas to the cathode catalyst layer

and thus shifts the occurrence of the performance drop to a higher value of the current

density. However, Fig. 3.12 (a) also shows that when the cathode gas diffusion layer

porosity reaches the value of 0.8, the cell performance almost does not change

comparing with the value of 0.7. This phenomenon also conform the result of Fig.

3.11. The variation of power density is also shown in Fig. 3.12 (b). It reveals that the

power density increases with the cathode gas diffusion layer porosity. In closing, if the

variation of solid phase conductivity is neglected, the cell performance is enhanced as

the cathode gas diffusion layer porosity increase. But when the cathode gas diffusion

layer porosity reaches the value of 0.7, the cell performance is not enhanced.

Figures 3.13 and 3.14 illustrate the same oxygen and water mass fractions at

various porosities of the cathode gas diffusion layer, respectively, in the direction of

the flow channel at an operating voltage of 0.7 V and a cathode relative humidity of

80%. According to the model equations, a higher porosity of gas diffusion layer

accelerates the speed of oxygen diffusion to the cathode catalyst layer, as displayed in

Fig. 3.13. Because of the aperture of the pores being relatively large, meaning that it

may not block by the liquid water and the diffusion transport of reactant gas is easy to

pass through the pores of gas diffusion layer. Hence, the oxygen does not spread

throughout the gas diffusion layer, and can reach the cathode catalyst layer. On the

contrary, the reactant gas spread throughout the gas diffusion layer for a small

porosity of gas diffusion layer. The diffusion transport of the reactant gas and the

liquid water by the capillary force to pass though the gas diffusion layer is difficult.

Fig. 3.13 also shows that when the porosity value is 0.7, no matter what the porosity is

increased, the oxygen mass fraction does not change obviously because of the fuel gas

or water almost pass though the gas diffusion layer directly. Figure 3.14 shows a

similar result with Fig 3.13. That is, the water moves though the gas diffusion layer

more easily at higher porosity of gas diffusion layer and the water does not

remarkably occupy the pores and thus preventing the oxygen diffusion transport.

3.7 Summary

An isothermal, multi-dimensional, multi-component, computational fluid

An isothermal, multi-dimensional, multi-component, computational fluid

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