• 沒有找到結果。

第五章 結論與建議

5.2 建議

1. FAIE 因動黏度較高故無法符合 CNS 15072 之標準,故若利用 IPA 為反應 醇類,則需使用動黏度較低之原油方可達到該標準之規範。

2. 油品之酸價、密度及動黏度皆會隨儲存時間而上升,故若要有較好之生質 柴油特性,則建議使用較新鮮之原油做為原料。

3. 若酯化反應後所得之油品生質柴油轉化率已超過 70 %,則在轉酯化反應時 可降低其醇油比,以達到減少 IPA 使用量之目的。

4. 超音波輔助系統在進行反應時,超音波探棒距離反應槽底部之距離不可太 遠,否則加熱及混合效果較差。

5. 進行高溫反應時,建議將 IPA 回收系統之冷凝水之水溫降低,亦或是延長 冷凝管之長度,以避免 IPA 及水蒸氣因高溫使得有部分未被收集,造成實

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驗之誤差。

6. 反應結束後進行水洗鹽析時,不可進行攪拌,以避免發生皂化反應,若發 生皂化反應將不利於油品之後續分析,並使整個生質柴油製造程序時間延 長。

7. 在進行轉酯化反應後由於含水率上升,在後續 NMR 分析時,會影響所得 到圖譜之正確性,並使得各不同 H 所對應在圖譜上之位置平移,故建議在 轉酯化反應後需先將水分去除後再進行 NMR 分析,以得到正確之生質柴 油轉化率。

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